Calcination of YBa2Cu3O7-x powder

K. C. Goretta; Ira Bloom; Nan Chen; G. T. Goudey; M. C. Hash; G. Klassen; M. T. Lanagan; R. B. Poeppel; J. P. Singh; Donglu Shi; U. Balachandran; J. T. Dusek; D. W. Capone

doi:10.1016/0167-577X(88)90001-8

Calcination of YBa₂Cu₃O_7-x powder

K. C. Goretta, Ira Bloom, Nan Chen, G. T. Goudey, M. C. Hash, G. Klassen, M. T. Lanagan, R. B. Poeppel, J. P. Singh, Donglu Shi, U. Balachandran, J. T. Dusek, D. W. Capone

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21 Scopus citations

Abstract

YBa₂Cu₃O_7-x was synthesized by mixed-oxide reaction of Y₂O₃, BaCO₃, and CuO. The starting constituents were mixed, followed by multiple steps of calcination with interposed grinding. Heating rapidly to 900°C was shown to minimize formation of liquid during calcination while still producing a phase-pure powder. Slow heating to 900°C or fast heating to 950°C resulted in formation of a liquid phase deleterious to YBa₂Cu₃O_7-x synthesis.

Original language	English (US)
Pages (from-to)	161-164
Number of pages	4
Journal	Materials Letters
Volume	7
Issue number	5-6
DOIs	https://doi.org/10.1016/0167-577X(88)90001-8
State	Published - Nov 1988

All Science Journal Classification (ASJC) codes

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1016/0167-577X(88)90001-8

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@article{3847d42cf93b4794b8ff10868d52130a,

title = "Calcination of YBa2Cu3O7-x powder",

abstract = "YBa2Cu3O7-x was synthesized by mixed-oxide reaction of Y2O3, BaCO3, and CuO. The starting constituents were mixed, followed by multiple steps of calcination with interposed grinding. Heating rapidly to 900°C was shown to minimize formation of liquid during calcination while still producing a phase-pure powder. Slow heating to 900°C or fast heating to 950°C resulted in formation of a liquid phase deleterious to YBa2Cu3O7-x synthesis.",

author = "Goretta, {K. C.} and Ira Bloom and Nan Chen and Goudey, {G. T.} and Hash, {M. C.} and G. Klassen and Lanagan, {M. T.} and Poeppel, {R. B.} and Singh, {J. P.} and Donglu Shi and U. Balachandran and Dusek, {J. T.} and Capone, {D. W.}",

note = "Funding Information: .j Work supported by the U.S. Department of Energy, Basic En-ergy Sciences - Materials Sciences, and the Office of Conser-vation and Renewable Energy, under contract W-3 lI09-ENG-38. {\textquoteright} Present address: Supercon. Inc.. Shrewsbury, MA 01545. USA.",

year = "1988",

month = nov,

doi = "10.1016/0167-577X(88)90001-8",

language = "English (US)",

volume = "7",

pages = "161--164",

journal = "Materials Letters",

issn = "0167-577X",

publisher = "Elsevier B.V.",

number = "5-6",

}

TY - JOUR

T1 - Calcination of YBa2Cu3O7-x powder

AU - Goretta, K. C.

AU - Bloom, Ira

AU - Chen, Nan

AU - Goudey, G. T.

AU - Hash, M. C.

AU - Klassen, G.

AU - Lanagan, M. T.

AU - Poeppel, R. B.

AU - Singh, J. P.

AU - Shi, Donglu

AU - Balachandran, U.

AU - Dusek, J. T.

AU - Capone, D. W.

N1 - Funding Information: .j Work supported by the U.S. Department of Energy, Basic En-ergy Sciences - Materials Sciences, and the Office of Conser-vation and Renewable Energy, under contract W-3 lI09-ENG-38. ’ Present address: Supercon. Inc.. Shrewsbury, MA 01545. USA.

PY - 1988/11

Y1 - 1988/11

N2 - YBa2Cu3O7-x was synthesized by mixed-oxide reaction of Y2O3, BaCO3, and CuO. The starting constituents were mixed, followed by multiple steps of calcination with interposed grinding. Heating rapidly to 900°C was shown to minimize formation of liquid during calcination while still producing a phase-pure powder. Slow heating to 900°C or fast heating to 950°C resulted in formation of a liquid phase deleterious to YBa2Cu3O7-x synthesis.

AB - YBa2Cu3O7-x was synthesized by mixed-oxide reaction of Y2O3, BaCO3, and CuO. The starting constituents were mixed, followed by multiple steps of calcination with interposed grinding. Heating rapidly to 900°C was shown to minimize formation of liquid during calcination while still producing a phase-pure powder. Slow heating to 900°C or fast heating to 950°C resulted in formation of a liquid phase deleterious to YBa2Cu3O7-x synthesis.

UR - http://www.scopus.com/inward/record.url?scp=0024106348&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0024106348&partnerID=8YFLogxK

U2 - 10.1016/0167-577X(88)90001-8

DO - 10.1016/0167-577X(88)90001-8

M3 - Article

AN - SCOPUS:0024106348

SN - 0167-577X

VL - 7

SP - 161

EP - 164

JO - Materials Letters

JF - Materials Letters

IS - 5-6

ER -

Calcination of YBa₂Cu₃O_7-x powder

Abstract

All Science Journal Classification (ASJC) codes

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