Electrostatic spinning, pyrolysis, and characterization of boron carbide nanofibers prepared from poly(norbornenyldecaborane) - A polymeric ceramic precursor

Daniel T. Welna; Xiaolan Wei; Jared D. Bender; Nick R. Krogman; Larry G. Sneddon; Harry R. Allcock

Electrostatic spinning, pyrolysis, and characterization of boron carbide nanofibers prepared from poly(norbornenyldecaborane) - A polymeric ceramic precursor

Daniel T. Welna, Xiaolan Wei, Jared D. Bender, Nick R. Krogman, Larry G. Sneddon, Harry R. Allcock

Research output: Contribution to journal › Conference article › peer-review

Abstract

Electrostatic spinning is a well-developed technique for the fabrication of fibers in the nanoscale domain. Novel boron carbide nanofibers were generated by the electrostatic spinning and ceramic conversion of poly(norbomenyldecaborane) (PND) - a polymeric ceramic precursor. The prepyrolyzed fibers were characterized by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy. The ceramic fibers were characterized by SEM, X-ray diffraction (XRD), B magic-angle spinning nuclear magnetic resonance (MAS NMR) and DRIFT spectroscopy. SEM analysis showed retention of the nanostructure in the pre- and postpyrolyzed fibers.

Original language	English (US)
Article number	FF6.13
Pages (from-to)	287-292
Number of pages	6
Journal	Materials Research Society Symposium Proceedings
Volume	848
State	Published - 2005
Event	2004 Materials Research Society Fall Meeting - Boston, MA, United States Duration: Nov 29 2004 → Dec 2 2004

All Science Journal Classification (ASJC) codes

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Cite this

@article{6efa9729af404caabd990b7194ce939f,

title = "Electrostatic spinning, pyrolysis, and characterization of boron carbide nanofibers prepared from poly(norbornenyldecaborane) - A polymeric ceramic precursor",

abstract = "Electrostatic spinning is a well-developed technique for the fabrication of fibers in the nanoscale domain. Novel boron carbide nanofibers were generated by the electrostatic spinning and ceramic conversion of poly(norbomenyldecaborane) (PND) - a polymeric ceramic precursor. The prepyrolyzed fibers were characterized by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy. The ceramic fibers were characterized by SEM, X-ray diffraction (XRD), B magic-angle spinning nuclear magnetic resonance (MAS NMR) and DRIFT spectroscopy. SEM analysis showed retention of the nanostructure in the pre- and postpyrolyzed fibers.",

author = "Welna, {Daniel T.} and Xiaolan Wei and Bender, {Jared D.} and Krogman, {Nick R.} and Sneddon, {Larry G.} and Allcock, {Harry R.}",

year = "2005",

language = "English (US)",

volume = "848",

pages = "287--292",

journal = "Materials Research Society Symposium Proceedings",

issn = "0272-9172",

publisher = "Materials Research Society",

note = "2004 Materials Research Society Fall Meeting ; Conference date: 29-11-2004 Through 02-12-2004",

}

Electrostatic spinning, pyrolysis, and characterization of boron carbide nanofibers prepared from poly(norbornenyldecaborane) - A polymeric ceramic precursor. / Welna, Daniel T.; Wei, Xiaolan; Bender, Jared D. et al.
In: Materials Research Society Symposium Proceedings, Vol. 848, FF6.13, 2005, p. 287-292.

Research output: Contribution to journal › Conference article › peer-review

TY - JOUR

T1 - Electrostatic spinning, pyrolysis, and characterization of boron carbide nanofibers prepared from poly(norbornenyldecaborane) - A polymeric ceramic precursor

AU - Welna, Daniel T.

AU - Wei, Xiaolan

AU - Bender, Jared D.

AU - Krogman, Nick R.

AU - Sneddon, Larry G.

AU - Allcock, Harry R.

PY - 2005

Y1 - 2005

N2 - Electrostatic spinning is a well-developed technique for the fabrication of fibers in the nanoscale domain. Novel boron carbide nanofibers were generated by the electrostatic spinning and ceramic conversion of poly(norbomenyldecaborane) (PND) - a polymeric ceramic precursor. The prepyrolyzed fibers were characterized by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy. The ceramic fibers were characterized by SEM, X-ray diffraction (XRD), B magic-angle spinning nuclear magnetic resonance (MAS NMR) and DRIFT spectroscopy. SEM analysis showed retention of the nanostructure in the pre- and postpyrolyzed fibers.

AB - Electrostatic spinning is a well-developed technique for the fabrication of fibers in the nanoscale domain. Novel boron carbide nanofibers were generated by the electrostatic spinning and ceramic conversion of poly(norbomenyldecaborane) (PND) - a polymeric ceramic precursor. The prepyrolyzed fibers were characterized by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy. The ceramic fibers were characterized by SEM, X-ray diffraction (XRD), B magic-angle spinning nuclear magnetic resonance (MAS NMR) and DRIFT spectroscopy. SEM analysis showed retention of the nanostructure in the pre- and postpyrolyzed fibers.

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M3 - Conference article

AN - SCOPUS:28844449336

SN - 0272-9172

VL - 848

SP - 287

EP - 292

JO - Materials Research Society Symposium Proceedings

JF - Materials Research Society Symposium Proceedings

M1 - FF6.13

T2 - 2004 Materials Research Society Fall Meeting

Y2 - 29 November 2004 through 2 December 2004

ER -

Electrostatic spinning, pyrolysis, and characterization of boron carbide nanofibers prepared from poly(norbornenyldecaborane) - A polymeric ceramic precursor

Abstract

All Science Journal Classification (ASJC) codes

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