Formation of highly textured BiSrCaCuO superconducting thick films by a rapid melting process

P. Prieto; G. Zorn; R. R. Arons; S. Thierfeldt; M. E. Gomez; B. Kabius; W. Sybertz; K. Urban

doi:10.1016/0038-1098(89)90841-7

Formation of highly textured BiSrCaCuO superconducting thick films by a rapid melting process

P. Prieto
, G. Zorn
, R. R. Arons
, S. Thierfeldt
, M. E. Gomez
, B. Kabius
, W. Sybertz
, K. Urban

Materials Research Institute (MRI)

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

We have prepared highly textured BiSrCaCuO thick films from mixtures of the oxides by a rapid melting process. Sample powders on (100)-MgO-substrates were melted within seconds and kept between 910 °C and 1050 °C for typically several minutes. The samples were then directly cooled to room temperature. The crystallization of Bi₂Sr₂CaCu₂O_x and the formation of a (001) - texture was observed in situ with a high-temperature X-ray diffractometer. Resistivity measurements showed the film to exhibit a T_c of 70 K. Subsequent annealing steps in air between 850 °C and 885 °C raised T_c to 85 K. The critical current density as inferred from magnetization measurements is at least 10³ A/cm². Morphology and composition of the films were investigated by scanning electron microscopy and electron diffraction.

Original language	English (US)
Pages (from-to)	235-240
Number of pages	6
Journal	Solid State Communications
Volume	69
Issue number	3
DOIs	https://doi.org/10.1016/0038-1098(89)90841-7
State	Published - Jan 1989

All Science Journal Classification (ASJC) codes

General Chemistry
Condensed Matter Physics
Materials Chemistry

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10.1016/0038-1098(89)90841-7

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@article{3e1ce37789ce42238005feda7b3bf933,

title = "Formation of highly textured BiSrCaCuO superconducting thick films by a rapid melting process",

abstract = "We have prepared highly textured BiSrCaCuO thick films from mixtures of the oxides by a rapid melting process. Sample powders on (100)-MgO-substrates were melted within seconds and kept between 910 °C and 1050 °C for typically several minutes. The samples were then directly cooled to room temperature. The crystallization of Bi2Sr2CaCu2Ox and the formation of a (001) - texture was observed in situ with a high-temperature X-ray diffractometer. Resistivity measurements showed the film to exhibit a Tc of 70 K. Subsequent annealing steps in air between 850 °C and 885 °C raised Tc to 85 K. The critical current density as inferred from magnetization measurements is at least 103 A/cm2. Morphology and composition of the films were investigated by scanning electron microscopy and electron diffraction.",

author = "P. Prieto and G. Zorn and Arons, \{R. R.\} and S. Thierfeldt and Gomez, \{M. E.\} and B. Kabius and W. Sybertz and K. Urban",

note = "Funding Information: Acknowledgements. The authors are grateful to H. Goebel, U. Poppe, B. Lengeler and J. Schubert for stimulating discussions. One of us (P.P.) wishes to thank the Alexander yon Humboldt Foundation for a fellowship in Germany.",

year = "1989",

month = jan,

doi = "10.1016/0038-1098(89)90841-7",

language = "English (US)",

volume = "69",

pages = "235--240",

journal = "Solid State Communications",

issn = "0038-1098",

publisher = "Elsevier Ltd",

number = "3",

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TY - JOUR

T1 - Formation of highly textured BiSrCaCuO superconducting thick films by a rapid melting process

AU - Prieto, P.

AU - Zorn, G.

AU - Arons, R. R.

AU - Thierfeldt, S.

AU - Gomez, M. E.

AU - Kabius, B.

AU - Sybertz, W.

AU - Urban, K.

N1 - Funding Information: Acknowledgements. The authors are grateful to H. Goebel, U. Poppe, B. Lengeler and J. Schubert for stimulating discussions. One of us (P.P.) wishes to thank the Alexander yon Humboldt Foundation for a fellowship in Germany.

PY - 1989/1

Y1 - 1989/1

N2 - We have prepared highly textured BiSrCaCuO thick films from mixtures of the oxides by a rapid melting process. Sample powders on (100)-MgO-substrates were melted within seconds and kept between 910 °C and 1050 °C for typically several minutes. The samples were then directly cooled to room temperature. The crystallization of Bi2Sr2CaCu2Ox and the formation of a (001) - texture was observed in situ with a high-temperature X-ray diffractometer. Resistivity measurements showed the film to exhibit a Tc of 70 K. Subsequent annealing steps in air between 850 °C and 885 °C raised Tc to 85 K. The critical current density as inferred from magnetization measurements is at least 103 A/cm2. Morphology and composition of the films were investigated by scanning electron microscopy and electron diffraction.

AB - We have prepared highly textured BiSrCaCuO thick films from mixtures of the oxides by a rapid melting process. Sample powders on (100)-MgO-substrates were melted within seconds and kept between 910 °C and 1050 °C for typically several minutes. The samples were then directly cooled to room temperature. The crystallization of Bi2Sr2CaCu2Ox and the formation of a (001) - texture was observed in situ with a high-temperature X-ray diffractometer. Resistivity measurements showed the film to exhibit a Tc of 70 K. Subsequent annealing steps in air between 850 °C and 885 °C raised Tc to 85 K. The critical current density as inferred from magnetization measurements is at least 103 A/cm2. Morphology and composition of the films were investigated by scanning electron microscopy and electron diffraction.

UR - https://www.scopus.com/pages/publications/0024482969

UR - https://www.scopus.com/pages/publications/0024482969#tab=citedBy

U2 - 10.1016/0038-1098(89)90841-7

DO - 10.1016/0038-1098(89)90841-7

M3 - Article

AN - SCOPUS:0024482969

SN - 0038-1098

VL - 69

SP - 235

EP - 240

JO - Solid State Communications

JF - Solid State Communications

IS - 3

ER -

Formation of highly textured BiSrCaCuO superconducting thick films by a rapid melting process

Abstract

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