Laboratory Investigation of Impact of Slickwater Composition on Multiphase Permeability Evolution in Tight Sandstones

Fracturing fluid filtrate that leaks off during injection is imbibed by strong capillary forces present in low-permeability sandstones and may severely reduce the effective gas permeability during cleanup and post-fracture production. This work aims to investigate the role fracturing fluid filtrate from slickwater has on rock-fluid and fluid-fluid interactions and to quantify the resulting multiphase permeability evolution during imbibition and drainage of the filtrate by means of specialized core laboratory techniques. Three suites of experiments were conducted. In the first suite of experiments, a fluid leakoff test was conducted on selected core samples to determine the extent of polymer invasion and leakoff characteristics. In the second suite, multigas relative permeability measurements were conducted on sandstone plugs saturated with fracturing fluid filtrate. A combination of controlled fluid evaporation and pulse decay permeability technique was used to measure liquid and gas effective permeabilities for both drainage and imbibition cycles. These experiments aim to capture dynamic permeability evolution during invasion and cleanup of fracturing fluid (slickwater). The final suite of experiments consists of adsorption flow tests to investigate, identify, and quantify possible mechanisms for adsorption of the polymeric molecules of friction reducers present in the fluid filtrate to the pore walls of the rock sample. Imbibition tests and observations of contact angles were conducted to validate possible wettability changes. Results from multiphase permeability flow tests show an irreversible reduction in endpoint brine permeability and relative permeability with increasing concentration of friction reducer. Our results also show that effective gas permeability during drainage/cleanup of the imbibed slickwater fluid is controlled to a large degree by trapped gas saturation than by changes in interfacial tension. Adsorption flow tests identified adsorption of polymeric molecules of the friction reducer present in the fluid to the pore walls of the rock. The adsorption friction reducer increases the wettability of the rock surface and results in the reduction of liquid relative permeability. The originality of this work is to diagnose formation damage mechanisms from laboratory experiments that adequately capture multiphase permeability evolution specific to a slickwater fluid system, during imbibition and cleanup. This will be useful in optimizing fracturing fluid selection.