Microwave-hydrothermal processing of titanium dioxide

Sridhar Komarneni; Rama K. Rajha; Hiroaki Katsuki

doi:10.1016/S0254-0584(99)00113-3

Microwave-hydrothermal processing of titanium dioxide

Sridhar Komarneni
, Rama K. Rajha
, Hiroaki Katsuki

Research output: Contribution to journal › Article › peer-review

166 Scopus citations

Abstract

Microwave-hydrothermal synthesis of titanium dioxide under various reaction conditions is reported. Crystallization of rutile from TiOCl₂ solutions was found to be extremely rapid. Titanium dioxide particle size, morphology and polymorph can be controlled by changing various parameters such as concentration, pH, pressure (or temperature), time and anionic species. The main advantages of microwave-hydrothermal processing of TiO₂ are (a) rapid heating to temperature and (b) extremely rapid kinetics of crystallization, both are expected to lead to energy savings.

Original language	English (US)
Pages (from-to)	50-54
Number of pages	5
Journal	Materials Chemistry and Physics
Volume	61
Issue number	1
DOIs	https://doi.org/10.1016/S0254-0584(99)00113-3
State	Published - Sep 30 1999

All Science Journal Classification (ASJC) codes

General Materials Science
Condensed Matter Physics

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@article{67245e80e6c54486acee140812aa94ae,

title = "Microwave-hydrothermal processing of titanium dioxide",

abstract = "Microwave-hydrothermal synthesis of titanium dioxide under various reaction conditions is reported. Crystallization of rutile from TiOCl2 solutions was found to be extremely rapid. Titanium dioxide particle size, morphology and polymorph can be controlled by changing various parameters such as concentration, pH, pressure (or temperature), time and anionic species. The main advantages of microwave-hydrothermal processing of TiO2 are (a) rapid heating to temperature and (b) extremely rapid kinetics of crystallization, both are expected to lead to energy savings.",

author = "Sridhar Komarneni and Rajha, \{Rama K.\} and Hiroaki Katsuki",

note = "Funding Information: This research was supported by the Materials Research Laboratory Consortium on Chemically Bonded Ceramics and Saga Ceramics Research Laboratory. Copyright: Copyright 2017 Elsevier B.V., All rights reserved.",

year = "1999",

month = sep,

day = "30",

doi = "10.1016/S0254-0584(99)00113-3",

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TY - JOUR

T1 - Microwave-hydrothermal processing of titanium dioxide

AU - Komarneni, Sridhar

AU - Rajha, Rama K.

AU - Katsuki, Hiroaki

N1 - Funding Information: This research was supported by the Materials Research Laboratory Consortium on Chemically Bonded Ceramics and Saga Ceramics Research Laboratory. Copyright: Copyright 2017 Elsevier B.V., All rights reserved.

PY - 1999/9/30

Y1 - 1999/9/30

N2 - Microwave-hydrothermal synthesis of titanium dioxide under various reaction conditions is reported. Crystallization of rutile from TiOCl2 solutions was found to be extremely rapid. Titanium dioxide particle size, morphology and polymorph can be controlled by changing various parameters such as concentration, pH, pressure (or temperature), time and anionic species. The main advantages of microwave-hydrothermal processing of TiO2 are (a) rapid heating to temperature and (b) extremely rapid kinetics of crystallization, both are expected to lead to energy savings.

AB - Microwave-hydrothermal synthesis of titanium dioxide under various reaction conditions is reported. Crystallization of rutile from TiOCl2 solutions was found to be extremely rapid. Titanium dioxide particle size, morphology and polymorph can be controlled by changing various parameters such as concentration, pH, pressure (or temperature), time and anionic species. The main advantages of microwave-hydrothermal processing of TiO2 are (a) rapid heating to temperature and (b) extremely rapid kinetics of crystallization, both are expected to lead to energy savings.

UR - https://www.scopus.com/pages/publications/0002649886

UR - https://www.scopus.com/pages/publications/0002649886#tab=citedBy

U2 - 10.1016/S0254-0584(99)00113-3

DO - 10.1016/S0254-0584(99)00113-3

M3 - Article

AN - SCOPUS:0002649886

SN - 0254-0584

VL - 61

SP - 50

EP - 54

JO - Materials Chemistry and Physics

JF - Materials Chemistry and Physics

IS - 1

ER -

Microwave-hydrothermal processing of titanium dioxide

Abstract

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