Microwave-hydrothermal synthesis of Fe-based materials for lithium-ion batteries and supercapacitors

Kunfeng Chen; Young Dong Noh; Wenyan Huang; Jianfeng Ma; Sridhar Komarneni; Dongfeng Xue

doi:10.1016/j.ceramint.2013.10.024

Microwave-hydrothermal synthesis of Fe-based materials for lithium-ion batteries and supercapacitors

Kunfeng Chen
, Young Dong Noh
, Wenyan Huang
, Jianfeng Ma
, Sridhar Komarneni
, Dongfeng Xue

Research output: Contribution to journal › Article › peer-review

25 Scopus citations

Abstract

Fe-based materials, Fe₂O₃, Fe₃O ₄, and FeOOH, were synthesized by the microwave-hydrothermal process in the temperature range of 100-200 C and under very short reaction times of 15 min to 2 h. Under microwave-controlled hydrolysis and redox reactions, cube-like Fe₂O₃ was crystallized using FeCl₃, Fe ₃O₄ particles were crystallized from FeCl₂ and FeOOH nanorods were crystallized using FeCl₃. The Fe-based materials were fabricated to make anodes and cathodes of lithium-ion battery and supercapacitor electrode materials to study their potential electrochemical applications. The electrochemical results showed that FeOOH had better anode capacity as lithium-ion batteries than those of Fe₂O₃ and Fe₃O₄. The present results suggest that the microwave-hydrothermally synthesized Fe-based materials are promising lithium-ion battery anode materials.

Original language	English (US)
Pages (from-to)	2877-2884
Number of pages	8
Journal	Ceramics International
Volume	40
Issue number	2
DOIs	https://doi.org/10.1016/j.ceramint.2013.10.024
State	Published - Mar 2014

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This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 7 Affordable and Clean Energy

All Science Journal Classification (ASJC) codes

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

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10.1016/j.ceramint.2013.10.024

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@article{7e735714f4874243a0ac64f84b9ea640,

title = "Microwave-hydrothermal synthesis of Fe-based materials for lithium-ion batteries and supercapacitors",

abstract = "Fe-based materials, Fe2O3, Fe3O 4, and FeOOH, were synthesized by the microwave-hydrothermal process in the temperature range of 100-200 C and under very short reaction times of 15 min to 2 h. Under microwave-controlled hydrolysis and redox reactions, cube-like Fe2O3 was crystallized using FeCl3, Fe 3O4 particles were crystallized from FeCl2 and FeOOH nanorods were crystallized using FeCl3. The Fe-based materials were fabricated to make anodes and cathodes of lithium-ion battery and supercapacitor electrode materials to study their potential electrochemical applications. The electrochemical results showed that FeOOH had better anode capacity as lithium-ion batteries than those of Fe2O3 and Fe3O4. The present results suggest that the microwave-hydrothermally synthesized Fe-based materials are promising lithium-ion battery anode materials.",

author = "Kunfeng Chen and \{Dong Noh\}, Young and Wenyan Huang and Jianfeng Ma and Sridhar Komarneni and Dongfeng Xue",

note = "Funding Information: Financial support from the National Natural Science Foundation of China (Grant nos. 50872016 , 20973033 and 51125009 ), the National Natural Science Foundation for Creative Research Group (Grant no. 21221061 ) and the Hundred Talents Program of the Chinese Academy of Sciences is acknowledged. Ms. Huang Wenyan gratefully acknowledges the financial sponsorship of Changzhou University Overseas Research and Training Program through an award. Dr. Ma Jianfeng gratefully acknowledges the financial sponsorship of Jiangsu Overseas Research and Training Program for University Prominent Young and Middle-aged Teachers and Presidents through an award. ",

year = "2014",

month = mar,

doi = "10.1016/j.ceramint.2013.10.024",

language = "English (US)",

volume = "40",

pages = "2877--2884",

journal = "Ceramics International",

issn = "0272-8842",

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T1 - Microwave-hydrothermal synthesis of Fe-based materials for lithium-ion batteries and supercapacitors

AU - Chen, Kunfeng

AU - Dong Noh, Young

AU - Huang, Wenyan

AU - Ma, Jianfeng

AU - Komarneni, Sridhar

AU - Xue, Dongfeng

N1 - Funding Information: Financial support from the National Natural Science Foundation of China (Grant nos. 50872016 , 20973033 and 51125009 ), the National Natural Science Foundation for Creative Research Group (Grant no. 21221061 ) and the Hundred Talents Program of the Chinese Academy of Sciences is acknowledged. Ms. Huang Wenyan gratefully acknowledges the financial sponsorship of Changzhou University Overseas Research and Training Program through an award. Dr. Ma Jianfeng gratefully acknowledges the financial sponsorship of Jiangsu Overseas Research and Training Program for University Prominent Young and Middle-aged Teachers and Presidents through an award.

PY - 2014/3

Y1 - 2014/3

N2 - Fe-based materials, Fe2O3, Fe3O 4, and FeOOH, were synthesized by the microwave-hydrothermal process in the temperature range of 100-200 C and under very short reaction times of 15 min to 2 h. Under microwave-controlled hydrolysis and redox reactions, cube-like Fe2O3 was crystallized using FeCl3, Fe 3O4 particles were crystallized from FeCl2 and FeOOH nanorods were crystallized using FeCl3. The Fe-based materials were fabricated to make anodes and cathodes of lithium-ion battery and supercapacitor electrode materials to study their potential electrochemical applications. The electrochemical results showed that FeOOH had better anode capacity as lithium-ion batteries than those of Fe2O3 and Fe3O4. The present results suggest that the microwave-hydrothermally synthesized Fe-based materials are promising lithium-ion battery anode materials.

AB - Fe-based materials, Fe2O3, Fe3O 4, and FeOOH, were synthesized by the microwave-hydrothermal process in the temperature range of 100-200 C and under very short reaction times of 15 min to 2 h. Under microwave-controlled hydrolysis and redox reactions, cube-like Fe2O3 was crystallized using FeCl3, Fe 3O4 particles were crystallized from FeCl2 and FeOOH nanorods were crystallized using FeCl3. The Fe-based materials were fabricated to make anodes and cathodes of lithium-ion battery and supercapacitor electrode materials to study their potential electrochemical applications. The electrochemical results showed that FeOOH had better anode capacity as lithium-ion batteries than those of Fe2O3 and Fe3O4. The present results suggest that the microwave-hydrothermally synthesized Fe-based materials are promising lithium-ion battery anode materials.

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M3 - Article

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SN - 0272-8842

VL - 40

SP - 2877

EP - 2884

JO - Ceramics International

JF - Ceramics International

IS - 2

ER -

Microwave-hydrothermal synthesis of Fe-based materials for lithium-ion batteries and supercapacitors

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