Processing of Pb(Zr0.52Ti0.48)O3 (PZT) ceramics from microwave and conventional hydrothermal powders

Isaac Robin Abothu; Shi Fang Liu; Sridhar Komarneni; Qing Hua Li

doi:10.1016/S0025-5408(99)00143-9

Processing of Pb(Zr_0.52Ti_0.48)O₃ (PZT) ceramics from microwave and conventional hydrothermal powders

Isaac Robin Abothu, Shi Fang Liu, Sridhar Komarneni, Qing Hua Li

Research output: Contribution to journal › Article › peer-review

32 Scopus citations

Abstract

Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.

Original language	English (US)
Pages (from-to)	1411-1419
Number of pages	9
Journal	Materials Research Bulletin
Volume	34
Issue number	9
DOIs	https://doi.org/10.1016/S0025-5408(99)00143-9
State	Published - Jul 1 1999

All Science Journal Classification (ASJC) codes

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

Access to Document

10.1016/S0025-5408(99)00143-9

Cite this

@article{565a57323fb7494aad94705338614526,

title = "Processing of Pb(Zr0.52Ti0.48)O3 (PZT) ceramics from microwave and conventional hydrothermal powders",

abstract = "Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.",

author = "Abothu, {Isaac Robin} and Liu, {Shi Fang} and Sridhar Komarneni and Li, {Qing Hua}",

year = "1999",

month = jul,

day = "1",

doi = "10.1016/S0025-5408(99)00143-9",

language = "English (US)",

volume = "34",

pages = "1411--1419",

journal = "Materials Research Bulletin",

issn = "0025-5408",

publisher = "Elsevier Ltd",

number = "9",

}

TY - JOUR

T1 - Processing of Pb(Zr0.52Ti0.48)O3 (PZT) ceramics from microwave and conventional hydrothermal powders

AU - Abothu, Isaac Robin

AU - Liu, Shi Fang

AU - Komarneni, Sridhar

AU - Li, Qing Hua

PY - 1999/7/1

Y1 - 1999/7/1

N2 - Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.

AB - Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.

UR - http://www.scopus.com/inward/record.url?scp=0001708076&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0001708076&partnerID=8YFLogxK

U2 - 10.1016/S0025-5408(99)00143-9

DO - 10.1016/S0025-5408(99)00143-9

M3 - Article

AN - SCOPUS:0001708076

SN - 0025-5408

VL - 34

SP - 1411

EP - 1419

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 9

ER -