Processing of Pb(Zr0.52Ti0.48)O3 (PZT) ceramics from microwave and conventional hydrothermal powders

Isaac Robin Abothu; Shi Fang Liu; Sridhar Komarneni; Qing Hua Li

doi:10.1016/S0025-5408(99)00143-9

Processing of Pb(Zr_0.52Ti_0.48)O₃ (PZT) ceramics from microwave and conventional hydrothermal powders

Isaac Robin Abothu
, Shi Fang Liu
, Sridhar Komarneni
, Qing Hua Li

Research output: Contribution to journal › Article › peer-review

33 Scopus citations

Abstract

Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.

Original language	English (US)
Pages (from-to)	1411-1419
Number of pages	9
Journal	Materials Research Bulletin
Volume	34
Issue number	9
DOIs	https://doi.org/10.1016/S0025-5408(99)00143-9
State	Published - Jul 1 1999

All Science Journal Classification (ASJC) codes

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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This output contributes to the following UN Sustainable Development Goals (SDGs)

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10.1016/S0025-5408(99)00143-9

Cite this

@article{565a57323fb7494aad94705338614526,

title = "Processing of Pb(Zr0.52Ti0.48)O3 (PZT) ceramics from microwave and conventional hydrothermal powders",

abstract = "Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95\% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.",

author = "Abothu, \{Isaac Robin\} and Liu, \{Shi Fang\} and Sridhar Komarneni and Li, \{Qing Hua\}",

year = "1999",

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doi = "10.1016/S0025-5408(99)00143-9",

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TY - JOUR

T1 - Processing of Pb(Zr0.52Ti0.48)O3 (PZT) ceramics from microwave and conventional hydrothermal powders

AU - Abothu, Isaac Robin

AU - Liu, Shi Fang

AU - Komarneni, Sridhar

AU - Li, Qing Hua

PY - 1999/7/1

Y1 - 1999/7/1

N2 - Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.

AB - Lead zirconium titanate (PZT) perovskite powders were synthesized without using any excess lead content by microwave hydrothermal method (M-H) at 122°C and conventional hydrothermal (C-H) method at 138°C. PZT powders prepared by both methods showed a particle size of less than 4 μm. Pellets prepared from these powders and sintered at 1250°C for 4 h, without any additives or sintering aids, showed densities in the range of 92-95% of theoretical density. Variation of relative permittivity and dissipation factor with temperature of these PZT pellets was studied. A maximum permittivity of 20,570, low dissipation factor of 0.002, and Curie temperature of 373°C were observed for sintered pellets prepared from PZT powders obtained by microwave hydrothermal method. The pellets prepared from PZT powders obtained by the conventional hydrothermal method showed a relative permittivity of 16,310, dissipation factor of 0.001, and Curie temperature of 351°C.

UR - https://www.scopus.com/pages/publications/0001708076

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