Simplified synthesis of micropore-free mesoporous silica, SBA-15, under microwave-hydrothermal conditions

Bharat L. Newalkar; Sridhar Komarneni

doi:10.1039/b202152h

Simplified synthesis of micropore-free mesoporous silica, SBA-15, under microwave-hydrothermal conditions

Bharat L. Newalkar, Sridhar Komarneni

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Abstract

Synthesis of micropore-free hydrothermally stable mesoporous silica SBA-15 has been accomplished by templating a silica precursor (sodium silicate/tetraethylorthosilicate) with pluronic123 copolymer (EO₂₀PO₇₀EO₂₀; M.W. 5,800) in the presence of cosolvent (ethanol) using a minimum salt (sodium chloride) content, under microwave-hydrothermal conditions at 373 K in 120 mins.

Original language	English (US)
Pages (from-to)	1774-1775
Number of pages	2
Journal	Chemical Communications
Volume	2
Issue number	16
DOIs	https://doi.org/10.1039/b202152h
State	Published - Jan 1 2002

All Science Journal Classification (ASJC) codes

Catalysis
Electronic, Optical and Magnetic Materials
Ceramics and Composites
General Chemistry
Surfaces, Coatings and Films
Metals and Alloys
Materials Chemistry

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10.1039/b202152h

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abstract = "Synthesis of micropore-free hydrothermally stable mesoporous silica SBA-15 has been accomplished by templating a silica precursor (sodium silicate/tetraethylorthosilicate) with pluronic123 copolymer (EO20PO70EO20; M.W. 5,800) in the presence of cosolvent (ethanol) using a minimum salt (sodium chloride) content, under microwave-hydrothermal conditions at 373 K in 120 mins.",

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AB - Synthesis of micropore-free hydrothermally stable mesoporous silica SBA-15 has been accomplished by templating a silica precursor (sodium silicate/tetraethylorthosilicate) with pluronic123 copolymer (EO20PO70EO20; M.W. 5,800) in the presence of cosolvent (ethanol) using a minimum salt (sodium chloride) content, under microwave-hydrothermal conditions at 373 K in 120 mins.

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Simplified synthesis of micropore-free mesoporous silica, SBA-15, under microwave-hydrothermal conditions

Abstract

All Science Journal Classification (ASJC) codes

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