Structural identification of a heterocyclic compound implicated in the Spanish toxic oil syndrome

G. S. Nomura; D. L. Ashley; A. H. Pendergrast; J. T. Bernert; D. G. Patterson; J. Grainger; D. Vanderveer

doi:10.1016/0278-6915(89)90065-3

Structural identification of a heterocyclic compound implicated in the Spanish toxic oil syndrome

G. S. Nomura, D. L. Ashley, A. H. Pendergrast, J. T. Bernert, D. G. Patterson, J. Grainger, D. Vanderveer

Forensic Science Program

Research output: Contribution to journal › Article › peer-review

4 Scopus citations

Abstract

The compound 1-phenyl-5-vinylimidazolidine-2-thione was previously reported to be the causative agent in the outbreak referred to as Spanish toxic oil syndrome. X-ray crystallography, together with nuclear magnetic resonance and infra-red spectroscopy, now show the correct structure of this compound to be N-(5-vinyl-1,3-thiazolidin-2-ylidene)phenylamine (5-VTPA). Data for the structural characterization of 5-VTPA and the closely related isomer N-(4-vinyl-1,3-thiazolidin-2-ylidene)phenylamine are reported.

Original language	English (US)
Pages (from-to)	165-171
Number of pages	7
Journal	Food and Chemical Toxicology
Volume	27
Issue number	3
DOIs	https://doi.org/10.1016/0278-6915(89)90065-3
State	Published - 1989

All Science Journal Classification (ASJC) codes

Food Science
Toxicology

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10.1016/0278-6915(89)90065-3

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title = "Structural identification of a heterocyclic compound implicated in the Spanish toxic oil syndrome",

abstract = "The compound 1-phenyl-5-vinylimidazolidine-2-thione was previously reported to be the causative agent in the outbreak referred to as Spanish toxic oil syndrome. X-ray crystallography, together with nuclear magnetic resonance and infra-red spectroscopy, now show the correct structure of this compound to be N-(5-vinyl-1,3-thiazolidin-2-ylidene)phenylamine (5-VTPA). Data for the structural characterization of 5-VTPA and the closely related isomer N-(4-vinyl-1,3-thiazolidin-2-ylidene)phenylamine are reported.",

author = "Nomura, {G. S.} and Ashley, {D. L.} and Pendergrast, {A. H.} and Bernert, {J. T.} and Patterson, {D. G.} and J. Grainger and D. Vanderveer",

year = "1989",

doi = "10.1016/0278-6915(89)90065-3",

language = "English (US)",

volume = "27",

pages = "165--171",

journal = "Food and Chemical Toxicology",

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T1 - Structural identification of a heterocyclic compound implicated in the Spanish toxic oil syndrome

AU - Nomura, G. S.

AU - Ashley, D. L.

AU - Pendergrast, A. H.

AU - Bernert, J. T.

AU - Patterson, D. G.

AU - Grainger, J.

AU - Vanderveer, D.

PY - 1989

Y1 - 1989

N2 - The compound 1-phenyl-5-vinylimidazolidine-2-thione was previously reported to be the causative agent in the outbreak referred to as Spanish toxic oil syndrome. X-ray crystallography, together with nuclear magnetic resonance and infra-red spectroscopy, now show the correct structure of this compound to be N-(5-vinyl-1,3-thiazolidin-2-ylidene)phenylamine (5-VTPA). Data for the structural characterization of 5-VTPA and the closely related isomer N-(4-vinyl-1,3-thiazolidin-2-ylidene)phenylamine are reported.

AB - The compound 1-phenyl-5-vinylimidazolidine-2-thione was previously reported to be the causative agent in the outbreak referred to as Spanish toxic oil syndrome. X-ray crystallography, together with nuclear magnetic resonance and infra-red spectroscopy, now show the correct structure of this compound to be N-(5-vinyl-1,3-thiazolidin-2-ylidene)phenylamine (5-VTPA). Data for the structural characterization of 5-VTPA and the closely related isomer N-(4-vinyl-1,3-thiazolidin-2-ylidene)phenylamine are reported.

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AN - SCOPUS:0024411515

SN - 0278-6915

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JO - Food and Chemical Toxicology

JF - Food and Chemical Toxicology

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ER -

Structural identification of a heterocyclic compound implicated in the Spanish toxic oil syndrome

Abstract

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