31P and 13C nmr measurements of a fructose-1-phosphate, Mn(II) and fructose 1,6-diphosphatase complex

S. J. Benkovic; J. J. Villafranca; J. J. Kleinschuster

doi:10.1016/0003-9861(73)90137-9

³¹P and ¹³C nmr measurements of a fructose-1-phosphate, Mn(II) and fructose 1,6-diphosphatase complex

S. J. Benkovic
, J. J. Villafranca
, J. J. Kleinschuster

Chemistry

Research output: Contribution to journal › Article › peer-review

11 Scopus citations

Abstract

Evidence for a ternary FDPase-Mn(II)-fructose-1-P complex is derived from ³¹P and ¹³C nmr measurements. Preliminary estimates of phosphorus and carbon to Mn(II) distances suggest that the oxygen at C-1 is coordinated to the metal ion in both the binary and ternary complex.

Original language	English (US)
Pages (from-to)	458-463
Number of pages	6
Journal	Archives of Biochemistry and Biophysics
Volume	155
Issue number	2
DOIs	https://doi.org/10.1016/0003-9861(73)90137-9
State	Published - Apr 1973

All Science Journal Classification (ASJC) codes

Biophysics
Biochemistry
Molecular Biology

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10.1016/0003-9861(73)90137-9

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title = "31P and 13C nmr measurements of a fructose-1-phosphate, Mn(II) and fructose 1,6-diphosphatase complex",

abstract = "Evidence for a ternary FDPase-Mn(II)-fructose-1-P complex is derived from 31P and 13C nmr measurements. Preliminary estimates of phosphorus and carbon to Mn(II) distances suggest that the oxygen at C-1 is coordinated to the metal ion in both the binary and ternary complex.",

author = "Benkovic, \{S. J.\} and Villafranca, \{J. J.\} and Kleinschuster, \{J. J.\}",

note = "Funding Information: 1 Supported in part by a research grant from the National Institutes of Health, GM 13306, and by a National Science Foundation Equipment Grant.",

year = "1973",

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journal = "Archives of Biochemistry and Biophysics",

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T1 - 31P and 13C nmr measurements of a fructose-1-phosphate, Mn(II) and fructose 1,6-diphosphatase complex

AU - Benkovic, S. J.

AU - Villafranca, J. J.

AU - Kleinschuster, J. J.

N1 - Funding Information: 1 Supported in part by a research grant from the National Institutes of Health, GM 13306, and by a National Science Foundation Equipment Grant.

PY - 1973/4

Y1 - 1973/4

N2 - Evidence for a ternary FDPase-Mn(II)-fructose-1-P complex is derived from 31P and 13C nmr measurements. Preliminary estimates of phosphorus and carbon to Mn(II) distances suggest that the oxygen at C-1 is coordinated to the metal ion in both the binary and ternary complex.

AB - Evidence for a ternary FDPase-Mn(II)-fructose-1-P complex is derived from 31P and 13C nmr measurements. Preliminary estimates of phosphorus and carbon to Mn(II) distances suggest that the oxygen at C-1 is coordinated to the metal ion in both the binary and ternary complex.

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U2 - 10.1016/0003-9861(73)90137-9

DO - 10.1016/0003-9861(73)90137-9

M3 - Article

C2 - 4350254

AN - SCOPUS:0015612146

SN - 0003-9861

VL - 155

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EP - 463

JO - Archives of Biochemistry and Biophysics

JF - Archives of Biochemistry and Biophysics

IS - 2

ER -

³¹P and ¹³C nmr measurements of a fructose-1-phosphate, Mn(II) and fructose 1,6-diphosphatase complex

Abstract

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