Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos)

Glenn S. Nomura; Donald G. Patterson

doi:10.1002/jlcr.2580360406

Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐¹³C₅‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos)

Glenn S. Nomura
, Donald G. Patterson

Forensic Science Program

Research output: Contribution to journal › Article › peer-review

Abstract

A stable isotope‐labelled analog of 3,5,6‐trichloropyridin‐2‐ol has been synthesized. 3,5,6‐Trichloropyridin‐2‐ol‐2,3,4,5,6‐¹³C₅‐¹⁵N was synthesized in a copper catalyzed cyclization from trichloroacetyl chloride‐1,2‐¹³C₂ and acrylonitrile‐1,2,3‐¹³C₃‐¹⁵N.

Original language	English (US)
Pages (from-to)	339-343
Number of pages	5
Journal	Journal of Labelled Compounds and Radiopharmaceuticals
Volume	36
Issue number	4
DOIs	https://doi.org/10.1002/jlcr.2580360406
State	Published - Apr 1995

All Science Journal Classification (ASJC) codes

Analytical Chemistry
Biochemistry
Radiology Nuclear Medicine and imaging
Drug Discovery
Spectroscopy
Organic Chemistry

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10.1002/jlcr.2580360406

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@article{daaca0336873450192456ceb04a6e086,

title = "Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos)",

abstract = "A stable isotope‐labelled analog of 3,5,6‐trichloropyridin‐2‐ol has been synthesized. 3,5,6‐Trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐15N was synthesized in a copper catalyzed cyclization from trichloroacetyl chloride‐1,2‐13C2 and acrylonitrile‐1,2,3‐13C3‐15N.",

author = "Nomura, \{Glenn S.\} and Patterson, \{Donald G.\}",

year = "1995",

month = apr,

doi = "10.1002/jlcr.2580360406",

language = "English (US)",

volume = "36",

pages = "339--343",

journal = "Journal of Labelled Compounds and Radiopharmaceuticals",

issn = "0362-4803",

publisher = "John Wiley and Sons Ltd",

number = "4",

}

Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐¹³C₅‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos). / Nomura, Glenn S.; Patterson, Donald G.
In: Journal of Labelled Compounds and Radiopharmaceuticals, Vol. 36, No. 4, 04.1995, p. 339-343.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos)

AU - Nomura, Glenn S.

AU - Patterson, Donald G.

PY - 1995/4

Y1 - 1995/4

N2 - A stable isotope‐labelled analog of 3,5,6‐trichloropyridin‐2‐ol has been synthesized. 3,5,6‐Trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐15N was synthesized in a copper catalyzed cyclization from trichloroacetyl chloride‐1,2‐13C2 and acrylonitrile‐1,2,3‐13C3‐15N.

AB - A stable isotope‐labelled analog of 3,5,6‐trichloropyridin‐2‐ol has been synthesized. 3,5,6‐Trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐15N was synthesized in a copper catalyzed cyclization from trichloroacetyl chloride‐1,2‐13C2 and acrylonitrile‐1,2,3‐13C3‐15N.

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UR - https://www.scopus.com/pages/publications/0028912364#tab=citedBy

U2 - 10.1002/jlcr.2580360406

DO - 10.1002/jlcr.2580360406

M3 - Article

AN - SCOPUS:0028912364

SN - 0362-4803

VL - 36

SP - 339

EP - 343

JO - Journal of Labelled Compounds and Radiopharmaceuticals

JF - Journal of Labelled Compounds and Radiopharmaceuticals

IS - 4

ER -

Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐¹³C₅‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos)

Abstract

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