Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique

Sorour Sadeghzade; Rahmatollah Emadi; Fariborz Tavangarian

doi:10.1007/978-3-030-36552-3_15

Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique

Sorour Sadeghzade, Rahmatollah Emadi, Fariborz Tavangarian

School of Science, Engineering & Technology (Harrisburg)

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

2 Scopus citations

Abstract

Hardystonite is currently recognized as a biocompatible bio-ceramic material for a range of medical applications. In this study, pure nanocrystalline hardystonite powder was prepared by mechanochemical synthesis of zinc oxide, silicate oxide, and egg shell in a planetary ball mill followed by sintering. It was found that pure nanocrystalline hardystonite powder formation occurred following 20 h of milling and subsequent sintering at 1000 ℃ for 3 h. Hardystonite scaffold was prepared by space holder method. The results showed that 3D porous scaffolds with pore sizes in the range of 200–300 μm, total and open porosity of 81 and 76%, respectively, with compressive strength and modulus of 0.35 and 10.49 MPa, were obtained. The average crystallite size of the prepared hardystonite powder and scaffold was measured to be 28 ± 3 and 79 ± 1 nm, respectively. The bioactivity of prepared scaffold was evaluated by simulated body fluid (SBF). Considering the results obtained, it seems that, manufactured scaffolds could be a good candidate for bone tissue engineering applications.

Original language	English (US)
Title of host publication	Advances in Powder and Ceramic Materials Science, TMS 2020
Editors	Bowen Li, Shefford P. Baker, Huazhang Zhai, Sergio Neves Monteiro, Rajiv Soman, Faqin Dong, Jinhong Li, Ruigang Wang
Publisher	Springer
Pages	143-150
Number of pages	8
ISBN (Print)	9783030365516
DOIs	https://doi.org/10.1007/978-3-030-36552-3_15
State	Published - 2020
Event	Symposium on Advances in Powder and Ceramic Material Science held at the 149th Annual Meeting and Exhibition, TMS 2020 - San Diego, United States Duration: Feb 23 2020 → Feb 27 2020

Publication series

Name	Minerals, Metals and Materials Series
ISSN (Print)	2367-1181
ISSN (Electronic)	2367-1696

Conference

Conference	Symposium on Advances in Powder and Ceramic Material Science held at the 149th Annual Meeting and Exhibition, TMS 2020
Country/Territory	United States
City	San Diego
Period	2/23/20 → 2/27/20

All Science Journal Classification (ASJC) codes

Electronic, Optical and Magnetic Materials
Energy Engineering and Power Technology
Mechanics of Materials
Metals and Alloys
Materials Chemistry

Access to Document

10.1007/978-3-030-36552-3_15

Cite this

Sadeghzade, S., Emadi, R., & Tavangarian, F. (2020). Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique. In B. Li, S. P. Baker, H. Zhai, S. N. Monteiro, R. Soman, F. Dong, J. Li, & R. Wang (Eds.), Advances in Powder and Ceramic Materials Science, TMS 2020 (pp. 143-150). (Minerals, Metals and Materials Series). Springer. https://doi.org/10.1007/978-3-030-36552-3_15

Sadeghzade, Sorour ; Emadi, Rahmatollah ; Tavangarian, Fariborz. / Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique. Advances in Powder and Ceramic Materials Science, TMS 2020. editor / Bowen Li ; Shefford P. Baker ; Huazhang Zhai ; Sergio Neves Monteiro ; Rajiv Soman ; Faqin Dong ; Jinhong Li ; Ruigang Wang. Springer, 2020. pp. 143-150 (Minerals, Metals and Materials Series).

@inproceedings{59fbc4cd4ab34563a870771a9275ec45,

title = "Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique",

abstract = "Hardystonite is currently recognized as a biocompatible bio-ceramic material for a range of medical applications. In this study, pure nanocrystalline hardystonite powder was prepared by mechanochemical synthesis of zinc oxide, silicate oxide, and egg shell in a planetary ball mill followed by sintering. It was found that pure nanocrystalline hardystonite powder formation occurred following 20 h of milling and subsequent sintering at 1000 ℃ for 3 h. Hardystonite scaffold was prepared by space holder method. The results showed that 3D porous scaffolds with pore sizes in the range of 200–300 μm, total and open porosity of 81 and 76%, respectively, with compressive strength and modulus of 0.35 and 10.49 MPa, were obtained. The average crystallite size of the prepared hardystonite powder and scaffold was measured to be 28 ± 3 and 79 ± 1 nm, respectively. The bioactivity of prepared scaffold was evaluated by simulated body fluid (SBF). Considering the results obtained, it seems that, manufactured scaffolds could be a good candidate for bone tissue engineering applications.",

author = "Sorour Sadeghzade and Rahmatollah Emadi and Fariborz Tavangarian",

note = "Publisher Copyright: {\textcopyright} 2020, The Minerals, Metals & Materials Society.; Symposium on Advances in Powder and Ceramic Material Science held at the 149th Annual Meeting and Exhibition, TMS 2020 ; Conference date: 23-02-2020 Through 27-02-2020",

year = "2020",

doi = "10.1007/978-3-030-36552-3_15",

language = "English (US)",

isbn = "9783030365516",

series = "Minerals, Metals and Materials Series",

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booktitle = "Advances in Powder and Ceramic Materials Science, TMS 2020",

}

Sadeghzade, S, Emadi, R & Tavangarian, F 2020, Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique. in B Li, SP Baker, H Zhai, SN Monteiro, R Soman, F Dong, J Li & R Wang (eds), Advances in Powder and Ceramic Materials Science, TMS 2020. Minerals, Metals and Materials Series, Springer, pp. 143-150, Symposium on Advances in Powder and Ceramic Material Science held at the 149th Annual Meeting and Exhibition, TMS 2020, San Diego, United States, 2/23/20. https://doi.org/10.1007/978-3-030-36552-3_15

Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique. / Sadeghzade, Sorour; Emadi, Rahmatollah; Tavangarian, Fariborz.
Advances in Powder and Ceramic Materials Science, TMS 2020. ed. / Bowen Li; Shefford P. Baker; Huazhang Zhai; Sergio Neves Monteiro; Rajiv Soman; Faqin Dong; Jinhong Li; Ruigang Wang. Springer, 2020. p. 143-150 (Minerals, Metals and Materials Series).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

TY - GEN

T1 - Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique

AU - Sadeghzade, Sorour

AU - Emadi, Rahmatollah

AU - Tavangarian, Fariborz

PY - 2020

Y1 - 2020

N2 - Hardystonite is currently recognized as a biocompatible bio-ceramic material for a range of medical applications. In this study, pure nanocrystalline hardystonite powder was prepared by mechanochemical synthesis of zinc oxide, silicate oxide, and egg shell in a planetary ball mill followed by sintering. It was found that pure nanocrystalline hardystonite powder formation occurred following 20 h of milling and subsequent sintering at 1000 ℃ for 3 h. Hardystonite scaffold was prepared by space holder method. The results showed that 3D porous scaffolds with pore sizes in the range of 200–300 μm, total and open porosity of 81 and 76%, respectively, with compressive strength and modulus of 0.35 and 10.49 MPa, were obtained. The average crystallite size of the prepared hardystonite powder and scaffold was measured to be 28 ± 3 and 79 ± 1 nm, respectively. The bioactivity of prepared scaffold was evaluated by simulated body fluid (SBF). Considering the results obtained, it seems that, manufactured scaffolds could be a good candidate for bone tissue engineering applications.

AB - Hardystonite is currently recognized as a biocompatible bio-ceramic material for a range of medical applications. In this study, pure nanocrystalline hardystonite powder was prepared by mechanochemical synthesis of zinc oxide, silicate oxide, and egg shell in a planetary ball mill followed by sintering. It was found that pure nanocrystalline hardystonite powder formation occurred following 20 h of milling and subsequent sintering at 1000 ℃ for 3 h. Hardystonite scaffold was prepared by space holder method. The results showed that 3D porous scaffolds with pore sizes in the range of 200–300 μm, total and open porosity of 81 and 76%, respectively, with compressive strength and modulus of 0.35 and 10.49 MPa, were obtained. The average crystallite size of the prepared hardystonite powder and scaffold was measured to be 28 ± 3 and 79 ± 1 nm, respectively. The bioactivity of prepared scaffold was evaluated by simulated body fluid (SBF). Considering the results obtained, it seems that, manufactured scaffolds could be a good candidate for bone tissue engineering applications.

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U2 - 10.1007/978-3-030-36552-3_15

DO - 10.1007/978-3-030-36552-3_15

M3 - Conference contribution

AN - SCOPUS:85079240979

SN - 9783030365516

T3 - Minerals, Metals and Materials Series

SP - 143

EP - 150

BT - Advances in Powder and Ceramic Materials Science, TMS 2020

A2 - Li, Bowen

A2 - Baker, Shefford P.

A2 - Zhai, Huazhang

A2 - Monteiro, Sergio Neves

A2 - Soman, Rajiv

A2 - Dong, Faqin

A2 - Li, Jinhong

A2 - Wang, Ruigang

PB - Springer

T2 - Symposium on Advances in Powder and Ceramic Material Science held at the 149th Annual Meeting and Exhibition, TMS 2020

Y2 - 23 February 2020 through 27 February 2020

ER -

Synthesis of Silicate Zinc Bioceramic via Mechanochemical Technique

Abstract

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All Science Journal Classification (ASJC) codes

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