Total synthesis and structure proof of (3E,8E)-suspensolide

Merle A. Battiste; James R. Rocca; Roman L. Wydra; James H. Tumlinson; Tatsuji Chuman

doi:10.1016/S0040-4039(00)82398-9

Total synthesis and structure proof of (3E,8E)-suspensolide

Merle A. Battiste
, James R. Rocca
, Roman L. Wydra
, James H. Tumlinson
, Tatsuji Chuman

Research output: Contribution to journal › Article › peer-review

31 Scopus citations

Abstract

A new macrolide, E,E-suspensolide (1), was prepared in six steps from mesityl oxide. The stereochemistries of intermediate isomers were assigned principally from their ¹³C NMR spectra. An isomeric macrolide, Z,E-suspensolide (2), was also prepared.

Original language	English (US)
Pages (from-to)	6565-6567
Number of pages	3
Journal	Tetrahedron Letters
Volume	29
Issue number	50
DOIs	https://doi.org/10.1016/S0040-4039(00)82398-9
State	Published - 1988

All Science Journal Classification (ASJC) codes

Biochemistry
Drug Discovery
Organic Chemistry

Access to Document

10.1016/S0040-4039(00)82398-9

Cite this

@article{7917dede6ba24a458f7bfd1856dfd2ef,

title = "Total synthesis and structure proof of (3E,8E)-suspensolide",

abstract = "A new macrolide, E,E-suspensolide (1), was prepared in six steps from mesityl oxide. The stereochemistries of intermediate isomers were assigned principally from their 13C NMR spectra. An isomeric macrolide, Z,E-suspensolide (2), was also prepared.",

author = "Battiste, \{Merle A.\} and Rocca, \{James R.\} and Wydra, \{Roman L.\} and Tumlinson, \{James H.\} and Tatsuji Chuman",

year = "1988",

doi = "10.1016/S0040-4039(00)82398-9",

language = "English (US)",

volume = "29",

pages = "6565--6567",

journal = "Tetrahedron Letters",

issn = "0040-4039",

publisher = "Elsevier Ltd",

number = "50",

}

TY - JOUR

T1 - Total synthesis and structure proof of (3E,8E)-suspensolide

AU - Battiste, Merle A.

AU - Rocca, James R.

AU - Wydra, Roman L.

AU - Tumlinson, James H.

AU - Chuman, Tatsuji

PY - 1988

Y1 - 1988

N2 - A new macrolide, E,E-suspensolide (1), was prepared in six steps from mesityl oxide. The stereochemistries of intermediate isomers were assigned principally from their 13C NMR spectra. An isomeric macrolide, Z,E-suspensolide (2), was also prepared.

AB - A new macrolide, E,E-suspensolide (1), was prepared in six steps from mesityl oxide. The stereochemistries of intermediate isomers were assigned principally from their 13C NMR spectra. An isomeric macrolide, Z,E-suspensolide (2), was also prepared.

UR - https://www.scopus.com/pages/publications/0013572943

UR - https://www.scopus.com/pages/publications/0013572943#tab=citedBy

U2 - 10.1016/S0040-4039(00)82398-9

DO - 10.1016/S0040-4039(00)82398-9

M3 - Article

AN - SCOPUS:0013572943

SN - 0040-4039

VL - 29

SP - 6565

EP - 6567

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 50

ER -

Total synthesis and structure proof of (3E,8E)-suspensolide

Abstract

All Science Journal Classification (ASJC) codes

Access to Document

Other files and links

Fingerprint

Cite this