ZSM-5 and ferrierite single crystals with lower Si/Al ratios: Synthesis and single-crystal synchrotron X-ray diffraction studies

Seok Han Kim; Sridhar Komarneni; Nam Ho Heo

doi:10.1016/j.micromeso.2011.02.010

ZSM-5 and ferrierite single crystals with lower Si/Al ratios: Synthesis and single-crystal synchrotron X-ray diffraction studies

Seok Han Kim, Sridhar Komarneni, Nam Ho Heo

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

Less twinned and high Al-containing ZSM-5 (MFI, Al_3.8Si _92.2O₁₉₂, Si/Al = 24.1) and high Al-containing ferrierite (FER, Al_2.0Si_34.0O₇₂, Si/Al = 16.7) large single crystals were synthesized by hydrothermal methods using mixed organic structure-directing agents and confirmed by single-crystal X-ray diffraction and SEM-EDX techniques. These large zeolite single crystals with an average size of 100 and 280 μm on an edge for ZSM-5 and ferrierite, respectively, were found to exhibit good qualities for potential use in advanced applications.

Original language	English (US)
Pages (from-to)	243-248
Number of pages	6
Journal	Microporous and Mesoporous Materials
Volume	143
Issue number	1
DOIs	https://doi.org/10.1016/j.micromeso.2011.02.010
State	Published - Aug 2011

All Science Journal Classification (ASJC) codes

General Chemistry
Condensed Matter Physics
Mechanics of Materials
General Materials Science

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10.1016/j.micromeso.2011.02.010

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title = "ZSM-5 and ferrierite single crystals with lower Si/Al ratios: Synthesis and single-crystal synchrotron X-ray diffraction studies",

abstract = "Less twinned and high Al-containing ZSM-5 (MFI, Al3.8Si 92.2O192, Si/Al = 24.1) and high Al-containing ferrierite (FER, Al2.0Si34.0O72, Si/Al = 16.7) large single crystals were synthesized by hydrothermal methods using mixed organic structure-directing agents and confirmed by single-crystal X-ray diffraction and SEM-EDX techniques. These large zeolite single crystals with an average size of 100 and 280 μm on an edge for ZSM-5 and ferrierite, respectively, were found to exhibit good qualities for potential use in advanced applications.",

author = "Kim, {Seok Han} and Sridhar Komarneni and Heo, {Nam Ho}",

year = "2011",

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doi = "10.1016/j.micromeso.2011.02.010",

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T1 - ZSM-5 and ferrierite single crystals with lower Si/Al ratios

T2 - Synthesis and single-crystal synchrotron X-ray diffraction studies

AU - Kim, Seok Han

AU - Komarneni, Sridhar

AU - Heo, Nam Ho

PY - 2011/8

Y1 - 2011/8

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AB - Less twinned and high Al-containing ZSM-5 (MFI, Al3.8Si 92.2O192, Si/Al = 24.1) and high Al-containing ferrierite (FER, Al2.0Si34.0O72, Si/Al = 16.7) large single crystals were synthesized by hydrothermal methods using mixed organic structure-directing agents and confirmed by single-crystal X-ray diffraction and SEM-EDX techniques. These large zeolite single crystals with an average size of 100 and 280 μm on an edge for ZSM-5 and ferrierite, respectively, were found to exhibit good qualities for potential use in advanced applications.

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ZSM-5 and ferrierite single crystals with lower Si/Al ratios: Synthesis and single-crystal synchrotron X-ray diffraction studies

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